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Title: | Microwave-assisted synthesis of 1,2,4- triazolo[4,3-a] [1,8]naphthyridines using FeCl3.6H2O under solvent-free conditions |
Authors: | Mogilaiah, K Prasad, R Shiva Swamy, J Kumara |
Keywords: | 1,2,4-Triazole;1,8-naphthyridine;FeCl3.6H2O;microwave irradiation;solvent-free conditions |
Issue Date: | Mar-2010 |
Publisher: | CSIR |
Abstract: | An efficient and convenient method for the synthesis of 9-aryl-6-(3-fluorophenyl)-1,2,4-triazolo[4,3-a][1,8]naphÂthyridines 8 from aryl aldehyde 3-(3-fluorophenyl)-1,8-naphthyridin-2-ylhydrazones 7 using FeCl3.6H2O under microwave irradiation is described. The yields are very good and purity is high. The structural assignments to these compounds are based on their spectral (IR, 1H NMR and MS) and analytical data. |
Page(s): | 335-339 |
Appears in Collections: | IJC-B Vol.49B(03) [March 2010] |
Files in This Item:
File | Description | Size | Format | |
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IJCB 49B(3) 335-339.pdf | 146.98 kB | Adobe PDF | View/Open |
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