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IJC-B Vol.49B(06) [June 2010] >

Title: Efficient synthesis of 1,3,4-oxadiazolyl-1,8-naphthyridines using iodobenzene diacetate in solid state
Authors: Mogilaiah, K
Kumar, K Shiva
Swamy, J Kumara
Chandra, A Vinay
Keywords: 1,3,4-Oxadiazoles
iodobenzene diacetate [ PhI(OAc)2]
solid state
Issue Date: Jun-2010
Publisher: CSIR
Abstract: A simple and highly efficient procedure has been described for the synthesis of 1-(5-aryl-[1,3,4]-oxadiazol-2-ylmethyl)-3-(3-methylphenyl)-1H-[1,8]naphthyridin-2-ones 5 by the oxidation of the corresponding [2-oxo-3-(3-methylphenyl)-2H-[1,8]naphthyri¬≠din-1-yl]acetic acid arylidenehydrazides 4 with iodobenzene diacetate [ PhI(OAc)2] in solid state. The products are obtained in good yields and in a state of high purity. The structural assignments of compounds 2-5 are based on their elemental analyses and spectral (IR and 1 H NMR) data.
Page(s): 840-844
Source:IJC-B Vol.49B(06) [June 2010]

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