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IJC-B Vol.49B [2010] >
IJC-B Vol.49B(06) [June 2010] >


Title: Facile one step synthesis of acyl azides and Nα –Fmoc/Boc/Z protected amino acid azides employing benzotriazole-1-yl-oxy-tris-(dimethylamino)-phosphonium hexafluorophosphate (BOP)
Authors: Vasantha, B
Sureshbabu, Vommina V
Keywords: One pot reaction
acyl azide
BOP
azidolysis
Issue Date: Jun-2010
Publisher: CSIR
Abstract: A simple route for the preparation of acyl azides from the corresponding carboxylic acids employing the peptide-coupling agent BOP is described. The procedure is simple, clean and high yielding. The chemistry is also extended to the preparation of several urethane protected amino acid azides (eight examples) as well.
Page(s): 812-817
Source:IJC-B Vol.49B(06) [June 2010]

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