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Title: Syntheses and spectral characterization of 2-aryloxy - 5,5'-bis(bromomethyl)-1,3,2-dioxaphosphorinane 2-oxides
Authors: Babu, M F Stephen
Anasuyamma, U
Venugopal, M
Raju, C Naga
Reddy, C Suresh
Issue Date: Jun-2005
Publisher: CSIR
IPC Code: Int.Cl.7 C 07 D
Abstract: 2-Aryloxy-5,5'-bis(bromomethyl)-1,3,2-dioxaphosphorinane 2-oxides 3 have been synthesized by the reaction of 2,2'-bis(bromomethyl)-1,3-propanediol 1 with various arylphosphorodichloridates 2a-h in the presence of triethylamine in dry tetrahydrofuran at room temperatuure. Their 1H, 13C,31P NMR and mass spectral data are discussed.
Page(s): 1248-1251
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.44B(06) [June 2005]

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