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Title: Syntheses and spectral characterization of 2-aryloxy - 5,5'-bis(bromomethyl)-1,3,2-dioxaphosphorinane 2-oxides
Authors: Babu, M F Stephen
Anasuyamma, U
Venugopal, M
Raju, C Naga
Reddy, C Suresh
Issue Date: Jun-2005
Publisher: CSIR
Series/Report no.: <b>Int</b>.<b>Cl</b>.<b><sup>7</sup> C 07 D</b>
Abstract: 2-Aryloxy-5,5'-bis(bromomethyl)-1,3,2-dioxaphosphorinane 2-oxides <b style="">3</b> have been synthesized by the reaction of 2,2'-bis(bromomethyl)-1,3-propanediol <b style="">1</b> with various arylphosphorodichloridates <b style="">2a-h</b> in the presence of triethylamine in dry tetrahydrofuran at room temperatuure. Their <sup>1</sup>H, <sup>13</sup>C,<sup>31</sup>P NMR and mass spectral data are discussed.
Description: 1248-1251
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.44B(06) [June 2005]

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