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|Title:||Synthesis of novel 2,' 3'-unsaturated nucleoside|
|Series/Report no.:||<b> Int</b>.<b>Cl</b>.<b><sup>7</sup> C 07 H</b>|
|Abstract:||5'-<i>tert</i>-Butyldimethylsilyl-5-iodo-6-methyluridine <b>1 </b>is converted to the bisxanthate <b>2</b> by reaction with carbon disulphide, followed by alkylation. The bisxanthate <b>2</b> on reduction with tri-<i>n</i>-butyltin hydride and desilylation affords the unsaturated nucleoside, 2',3'-didehydro-2',3'-dideoxy-5-iodo-6-methyluridine <b>4</b>.|
|Appears in Collections:||IJC-B Vol.44B(05) [May 2005]|
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