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IJC-B Vol.44B [2005] >
IJC-B Vol.44B(01) [January 2005] >

Title: Solvent-free synthesis of 2′,3′,5′-tri-O-acetyl -2,6-dichloropurine nucleoside catalyzed by p-toluenesulfonic acid using microwave
Authors: Qu, Guirong
Liu, Qibin
Issue Date: Jan-2005
Publisher: CSIR
IPC CodeInt.Cl.7 C 07 D 473/00
Abstract: Starting from tetraacetylribofuranose 1 and 2,6-dichloropurine 2, in the presence of p-toluenesulfonic acid (p-TsOH), 2′,3′,5′-tri-O-acetyl-2,6-dichloropurine nucleoside 3 has been synthesized in microwave oven for the first time. On comparing(→ Comparing) with the conventional methods, this method has advantages such as shorter reaction time (4.5min), better yield (83.5%), simple(→simpler) workup and environmental acceptability.
Page(s): 196-197
ISSN: 0975-0983(Online); 0376-4699(Print)
Source:IJC-B Vol.44B(01) [January 2005]

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