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Title: Soft hydrothermal synthesis, morphology and characterization of disodium nickel pyrophosphate crystals: Na2NiP2O7
Authors: Mahesh, M J
Gopalakrishna, G S
Ashamanjari, K G
Keywords: Hydrothermal synthesis;Solubility;Morphology;Magnetic property
Issue Date: Dec-2005
Publisher: CSIR
IPC Code: C3/0B
Abstract: Na2NiP2O7 crystals were synthesized by soft hydrothermal rout at moderate pressure-temperature conditions. Highest degree of crystallinity observed at critical concentration of initial components and beyond which the crystallinity collapse sharply to minimum. Solubility studies revealed positive thermal coefficient with relatively high enthalpy in H3PO4. Magnetic results indicated that it is a frequency dependent paramagnetic material.
Page(s): 952-957
ISSN: 0975-1041 (Online); 0019-5596 (Print)
Appears in Collections:IJPAP Vol.43(12) [December 2005]

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