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Title: Synthesis, crystal structure and study of X-H…A interactions in<b style=""> </b>N,N′-bis-(4-methoxy-benzylidine)-hydrazine
Authors: Rajnikant
Deshmukh, M. B.
Keywords: Crystal structure
Intra- and Intermolecular Interactions
Issue Date: Aug-2006
Publisher: CSIR
Series/Report no.: B28D5/00
Abstract: Synthesis and crystal structure of N,N′-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters <i style="">a</i> = 17.416(3), <i style="">b</i> = 10.711(3) and <i style="">c </i>=8.428(3)Å, <img src='/image/spc_char/beta.gif' border=0> =113.64(2)<sup>o</sup>, <i style="">V</i> = 1440.2(8)Å<sup>3 </sup>and <i style="">Z</i> = 4. The structure has been refined to a <i style="">R</i>-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions.
Description: 602-605
ISSN: 0975-1041 (Online); 0019-5596 (Print)
Appears in Collections:IJPAP Vol.44(08) [August 2006]

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