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IJPAP Vol.44(08) [August 2006] >


Title: Synthesis, crystal structure and study of X-H…A interactions in N,N′-bis-(4-methoxy-benzylidine)-hydrazine
Authors: Rajnikant
Dinesh
Deshmukh, M. B.
Kamni
Keywords: Crystal structure
Hydrazines
Intra- and Intermolecular Interactions
Alkaloid
Issue Date: Aug-2006
Publisher: CSIR
IPC CodeB28D5/00
Abstract: Synthesis and crystal structure of N,N′-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters a = 17.416(3), b = 10.711(3) and c =8.428(3)Å, =113.64(2)o, V = 1440.2(8)Å3 and Z = 4. The structure has been refined to a R-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions.
Page(s): 602-605
ISSN: 0975-1041 (Online); 0019-5596 (Print)
Source:IJPAP Vol.44(08) [August 2006]

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