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|Title:||Synthesis, crystal structure and study of X-H…A interactions in N,N′-bis-(4-methoxy-benzylidine)-hydrazine|
Deshmukh, M. B.
|Keywords:||Crystal structure;Hydrazines;Intra- and Intermolecular Interactions;Alkaloid|
|Abstract:||Synthesis and crystal structure of N,N′-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters a = 17.416(3), b = 10.711(3) and c =8.428(3)Å, =113.64(2)o, V = 1440.2(8)Å3 and Z = 4. The structure has been refined to a R-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions.|
|ISSN:||0975-1041 (Online); 0019-5596 (Print)|
|Appears in Collections:||IJPAP Vol.44(08) [August 2006]|
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