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IJC-B Vol.46B(10) [October 2007] >

Title: Synthesis and studies of some novel s-triazine based aminopyrimidines, isoxazoles and 1,5-benzothiazepines
Authors: Solankee, Anjani
Kapadia, Kishor
Solankee, Pankit
Prajapati, Yogesh
Patel, Hiral
Solankee, Sejal
Keywords: Aminopyrimidines
Glacial acetic acid
s-triazine nucleus
Issue Date: Oct-2007
Publisher: CSIR
Abstract: An elegant synthesis of the titled compounds 7a-e, 8a-e and 9a-e have been presented starting from chalcones 6a-e based on s-triazine nucleus. These chalcones 6a-e on cyclisation with guanidine nitrate and hydroxylamine hydrochloride in the presence of alkali give aminopyrimidines 7a-e and isoxazoles 8a-e respectively. Further these chalcones 6a-e on cyclisation with 2-aminothiophenol in the presence of few drops of glacial acetic acid give 1,5-benzothiazepines 9a-e. All the products obtained from these reactions are characterized by elemental analysis, IR, ¹H NMR and mass spectral data.
Page(s): 1707-1712
ISSN: 0376-4699
Source:IJC-B Vol.46B(10) [October 2007]

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