NISCAIR Online Periodicals Repository

Research Journals >
Journal of Scientific and Industrial Research (JSIR) >
JSIR Vol.69 [2010] >
JSIR Vol.69(03) [March 2010] >

Title: Synthesis and characterization of methyl nitramino -2, 4, 6-trinitrobenzenes using bismuth nitrate pentahydrate as an eco friendly nitrating agent
Authors: Badgujar, D M
Talawar, M B
Asthana, S N
Mahulikar, P P
Keywords: Bismuth nitrate
Eco-friendly nitration
Microwave irradiation
Issue Date: Mar-2010
Publisher: CSIR
Abstract: This study presents synthesis of 2,4,6-trinitrophenylmethyl- nitramine (3a) 2,4,6-trinitro-1,3-di(methylnitramino) benzene (3b) and 2,4,6-trinitro-1,3,5-tris(methylnitramino) benzene (3c) by nitration of 2,4,6-trinitro-N-methylaniline (2a), 2,4,6-trinitro- 1,3-di(methylamino) benzene (2b) and 2,4,6-trinitro-1,3,5-tris(methylamino) benzene (2c) using bismuth nitrate pentahydrate in tetrahydrofuran adsorbed on silica gel and fly ash as solid supports under microwave irradiation. An eco-friendly nitration approach used in synthesis of target compounds (3a-3c) is of interest for the production of high energy materials.
Page(s): 208-210
ISSN: 0975-1084 (Online); 0022-4456 (Print)
Source:JSIR Vol.69(03) [March 2010]

Files in This Item:

File Description SizeFormat
JSIR 69(3) 208-210.pdf53.56 kBAdobe PDFView/Open
 Current Page Visits: 965 
Recommend this item


Online Submission of Articles |  NISCAIR Website |  National Knowledge Resources Consortium |  Contact us |  Feedback

Disclaimer: NISCAIR assumes no responsibility for the statements and opinions advanced by contributors. The editorial staff in its work of examining papers received for publication is helped, in an honorary capacity, by many distinguished engineers and scientists.

CC License Except where otherwise noted, the Articles on this site are licensed under Creative Commons License: CC Attribution-Noncommercial-No Derivative Works 2.5 India

Copyright © 2015 The Council of Scientific and Industrial Research, New Delhi. All rights reserved.

Powered by DSpace Copyright © 2002-2007 MIT and Hewlett-Packard | Compliant to OAI-PMH V 2.0

Home Page Total Visits: 169087 since 01-Sep-2015  Last updated on 29-Jun-2016Webmaster: