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Title: The electrosynthesis of pinacols
Authors: Jiang Bian, Yan-
Sheng Bai, Dong-
Keywords: Pinacols;Electrosynthesis;Iron;Electrode;Aqueous
Issue Date: Nov-2007
Publisher: CSIR
Abstract: Electrosynthesis of pinacols by iron as electrode in acid condi-tion is performed. The influence of electric potential and time on pinacol yield is explored. The optimal reaction conditions are at electric potential 4 V, time 60 min., methanol (6 mL), hydrochlo-ric acid (2 N, 2 mL), with the yield of pinacols up to 18-81%. The main advantages of the present procedure are milder reaction conditions and operational simplicity.
Page(s): 1890-1892
ISSN: 0376-4699
Appears in Collections:IJC-B Vol.46B(11) [November 2007]

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