Please use this identifier to cite or link to this item:
http://nopr.niscair.res.in/handle/123456789/719| Title: | The electrosynthesis of pinacols |
| Authors: | Jiang Bian, Yan- Sheng Bai, Dong- |
| Keywords: | Pinacols;Electrosynthesis;Iron;Electrode;Aqueous |
| Issue Date: | Nov-2007 |
| Publisher: | CSIR |
| Abstract: | Electrosynthesis of pinacols by iron as electrode in acid condi-tion is performed. The influence of electric potential and time on pinacol yield is explored. The optimal reaction conditions are at electric potential 4 V, time 60 min., methanol (6 mL), hydrochlo-ric acid (2 N, 2 mL), with the yield of pinacols up to 18-81%. The main advantages of the present procedure are milder reaction conditions and operational simplicity. |
| Page(s): | 1890-1892 |
| URI: | http://hdl.handle.net/123456789/719 |
| ISSN: | 0376-4699 |
| Appears in Collections: | IJC-B Vol.46B(11) [November 2007] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCB 46B(11) (2007) 1890-1892.pdf | 148.64 kB | Adobe PDF | View/Open |
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