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Title: Synthesis of 1,3,5-triazinane-2-thiones and 1,3,5-oxadiazinane-4-thiones linked with isoxazoles
Authors: Rajanarendar, E
Reddy, A Siva Rami
Shaik, Firoz Pasha
Keywords: Isoxazolyl trizinane-2-thiones
trimolecular condensa­tion
isoxazolyl oxadiazinane-4-thiones
Issue Date: Jan-2010
Publisher: CSIR
Abstract: <smarttagtype namespaceuri="urn:schemas-microsoft-com:office:smarttags" name="metricconverter"> Trimolecular condensation of <i>N</i>-(3,5-dimethyl-4-isoxazolyl)-<i>N</i>'-arylthioureas <b>2 </b>obtained from<b> 1</b> by reaction with aryliso­thiocyanates, with aqueous formaldehyde and primary amines in toluene under reflux leads to 5-alkyl-1-(3,5-dimethyl-4-iso­xa­zolyl)-3-aryl-hexahydro-1,3,5-triazinane-2-thiones<b> 3 </b>in excellent yields. Condensation of <b>2 </b>with aqueous formaldehyde under similar condition provides isoxazolyl 1,3,5-oxadiazinane-4-thiones <b style="">4</b>. </smarttagtype>
Description: 119-122
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.49B(01) [January 2010]

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