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IJC-B Vol.49B(01) [January 2010] >

Title: Synthesis of 1,3,5-triazinane-2-thiones and 1,3,5-oxadiazinane-4-thiones linked with isoxazoles
Authors: Rajanarendar, E
Reddy, A Siva Rami
Shaik, Firoz Pasha
Keywords: Isoxazolyl trizinane-2-thiones
trimolecular condensa­tion
isoxazolyl oxadiazinane-4-thiones
Issue Date: Jan-2010
Publisher: CSIR
Abstract:  Trimolecular condensation of N-(3,5-dimethyl-4-isoxazolyl)-N'-arylthioureas 2 obtained from 1 by reaction with aryliso­thiocyanates, with aqueous formaldehyde and primary amines in toluene under reflux leads to 5-alkyl-1-(3,5-dimethyl-4-iso­xa­zolyl)-3-aryl-hexahydro-1,3,5-triazinane-2-thiones 3 in excellent yields. Condensation of 2 with aqueous formaldehyde under similar condition provides isoxazolyl 1,3,5-oxadiazinane-4-thiones 4.
Page(s): 119-122
ISSN: 0975-0983(Online); 0376-4699(Print)
Source:IJC-B Vol.49B(01) [January 2010]

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