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IJC-B Vol.45B(08) [August 2006] >


Title: A new route to the synthesis of long-chain methyl -chlorooxoalkanoates
Authors: Rauf, Abdul
Ahmad, Shabana
Keywords: Methyl epoxyalkanoates
chlorotrimethylsilane
Jones′ oxidation
methyl -chlorooxoalkanoates
Issue Date: Aug-2006
Publisher: CSIR
IPC CodeInt.Cl.8 C07C
Abstract: A reaction of long-chain methyl epoxyalkanoates with chlorotrimethylsilane in presence of triethylamine followed by Jones oxidation has resulted in the formation of respective chlorooxo derivatives. The reaction proceeds under mild conditions and in a short span of time. Thus, one pot synthesis of methyl chlorooxoalkanoates is assisted with high purity and good yield of the products. The pure products are characterized by IR, 1H NMR, 13C NMR and MS spectra.
Page(s): 1924-1928
ISSN: 0975-0983(Online); 0376-4699(Print)
Source:IJC-B Vol.45B(08) [August 2006]

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