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Indian Journal of Chemistry -Section B (IJC-B) >
IJC-B Vol.45B [2006] >
IJC-B Vol.45B(01) [January 2006] >
| Title: | A simple method for deprotection of tert-butyldimethylsilyl ethers by using stannous chloride under microwave irradiation |
| Authors: | Jadhav, Vinod H
Borate, Hanumant B
Wakharkar, Radhika D |
| Keywords: | tert-Butyldimethylsilyl ethers
stannous chloride
deprotection
microwave |
| Issue Date: | Jan-2006 |
| Publisher: | CSIR |
| IPC Code: | Int.Cl.7 C 07 C |
| Abstract: | A facile regeneration of hydroxy compounds from their tert-butyldimethylsilyl ethers in presence of stannous chloride under solvent free conditions using domestic microwave oven has been performed efficiently in a short period (5-6 min). The conversion using stannous chloride in ethanol or water for comparison of the efficiency has been described. The generality of the transformation has been confirmed by several examples. |
| Page(s): | 322-324 |
| ISSN: | 0975-0983(Online); 0376-4699(Print) |
| Source: | IJC-B Vol.45B(01) [January 2006]
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