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Title: A simple method for deprotection of tert-butyldimethylsilyl ethers by using stannous chloride under microwave irradiation
Authors: Jadhav, Vinod H
Borate, Hanumant B
Wakharkar, Radhika D
Keywords: tert-Butyldimethylsilyl ethers;stannous chloride;deprotection;microwave
Issue Date: Jan-2006
Publisher: CSIR
IPC Code: Int.Cl.7 C 07 C
Abstract: A facile regeneration of hydroxy compounds from their tert-butyldimethylsilyl ethers in presence of stannous chloride under solvent free conditions using domestic microwave oven has been performed efficiently in a short period (5-6 min). The conversion using stannous chloride in ethanol or water for comparison of the efficiency has been described. The generality of the transformation has been confirmed by several examples.
Page(s): 322-324
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.45B(01) [January 2006]

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