Please use this identifier to cite or link to this item:
Title: A simple method for deprotection of tert-butyldimethylsilyl ethers by using stannous chloride under microwave irradiation
Authors: Jadhav, Vinod H
Borate, Hanumant B
Wakharkar, Radhika D
Keywords: tert-Butyldimethylsilyl ethers
stannous chloride
Issue Date: Jan-2006
Publisher: CSIR
Series/Report no.: Int.Cl.7 C 07 C
Abstract: A facile regeneration of hydroxy compounds from their tert-butyldimethylsilyl ethers in presence of stannous chloride under solvent free conditions using domestic microwave oven has been performed efficiently in a short period (5-6 min). The conversion using stannous chloride in ethanol or water for comparison of the efficiency has been described. The generality of the transformation has been confirmed by several examples.
Description: 322-324
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.45B(01) [January 2006]

Files in This Item:
File Description SizeFormat 
IJCB 45B(1) 322-324.pdf36.4 kBAdobe PDFView/Open

Items in NOPR are protected by copyright, with all rights reserved, unless otherwise indicated.