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Title: Synthesis and characterisation of Sb₂Zn₂Cl₄ (OPri)₆, MSb₂Cl₂ (OPri)₆ (M = Be, Mg, Zn), and M₂Ti₄Cl₄(OPri)₁₆ (M = Mg, Zn)
Authors: Shahani, Jayshree
Singh, Anirudh
Issue Date: Jan-2008
Publisher: CSIR
IPC Code: Int. Cl. ⁸ C07F3/00; C07F3/02; C07F3/06; C07F7/28; C07F9/90
Abstract: Reactions of MCl2 (M = Be, Mg, Zn) with Sb(OPri)₃ and Ti(OPri)₄ in desired molar ratios in benzene afford structurally interesting derivatives of the types MSb₂Cl₂ (OPri)₆ (M Be(1), Mg(2), Zn(3)), Sb₂Zn₂Cl₄(OPri)₆(4), M₂Ti₄Cl₄(OPri)₁₆ (M = Mg(5), Zn(6)). All these derivatives have been characterized by elemental (Be, Mg, Zn, Sb, Cl, Ti) analyses, isopropoxo groups determinations, molecular weight measurements, and spectro-scopic studies.
Page(s): 55-57
ISSN: 0376-4710
Appears in Collections:IJC-A Vol.47A(01) [January 2008]

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