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IJC-B Vol.48B(07) [July 2009] >

Title: Synthesis and characterization of fused and spiro heterocycles by ultrasonic methods
Authors: Dabholkar, Vijay V
Wadkar, Mihir M
Keywords: Thiazole
Issue Date: Jul-2009
Publisher: CSIR
Abstract: Treatment of 1,4-diazacyclohexan-2,5-dione 1 with bromine in carbon tetrachloride has yielded 1,4-diaza-3-bromo-2,5-dioxocyclo­hexane 2 and 1,4-diaza-3,3-dibromocyclohexane-2,5-dione 7. The reaction of 2 with carbamides/thiocarbamides has produced 6-oxo-oxazolo[4,5-b] piperazine 5 /2-substituted imino-6-oxo-thia­zolo­[4,5-b] piperazine 6. Compound 7 on combination with carba­mides/ thiocarbamides is transformed to 1-oxo-2-substi­tuted imino-3,5,8-triaza-3H,5H,8H,7-dihydro-6,9-dioxo-spiro [3.5] non­­ane 9 and 1-thia-2-substituted imino-3,5,8-triaza-3H,5H,8H-7dihydro-6,9-dioxo-spiro [3.5] nonane 9. The structures of the synthesized compounds have been confirmed by IR, 1H and 13C NMR spectral data analyses.
Page(s): 1027-1032
ISSN: 0975-0983 (Online); 0376-4699 (Print)
Source:IJC-B Vol.48B(07) [July 2009]

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