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http://nopr.niscair.res.in/handle/123456789/4547| Title: | 1H, 13C, 2D NMR and GCMS characterization of diol derivatives |
| Authors: | Manivel, P Khan, F Nawaz |
| Keywords: | Isocoumarins;diols;NaBH4;2D NMR;GCMS |
| Issue Date: | Jun-2009 |
| Publisher: | CSIR |
| Abstract: | Sodium borohydride (SBH) reduction of isocoumarins has been effected in presence of methanol to their respective diols. Diols have been isolated, purified and characterized by GCMS, proton, carbon and two-dimensional NMR spectroscopy analysis. Complete NMR assignments of diols are made using H–H COSY, as well as HSQC, HMQC and HMBC heteronuclear correlation techniques. |
| Page(s): | 825-832 |
| URI: | http://hdl.handle.net/123456789/4547 |
| ISSN: | 0376-4699 |
| Appears in Collections: | IJC-B Vol.48B(06) [June 2009] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCB 48B(6) 825-832.pdf | 197.69 kB | Adobe PDF | View/Open |
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