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Title: 1H, 13C, 2D NMR and GCMS characterization of diol derivatives
Authors: Manivel, P
Khan, F Nawaz
Keywords: Isocoumarins;diols;NaBH4;2D NMR;GCMS
Issue Date: Jun-2009
Publisher: CSIR
Abstract: Sodium borohydride (SBH) reduction of isocoumarins has been effected in presence of methanol to their respective diols. Diols have been isolated, purified and characterized by GCMS, proton, carbon and two-dimensional NMR spectroscopy analysis. Complete NMR assignments of diols are made using H–H COSY, as well as HSQC, HMQC and HMBC heteronuclear correlation techniques.
Page(s): 825-832
ISSN: 0376-4699
Appears in Collections:IJC-B Vol.48B(06) [June 2009]

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