Please use this identifier to cite or link to this item: http://nopr.niscair.res.in/handle/123456789/4547
Title: 1H, 13C, 2D NMR and GCMS characterization of diol derivatives
Authors: Manivel, P
Khan, F Nawaz
Keywords: Isocoumarins
diols
NaBH4
2D NMR
GCMS
Issue Date: Jun-2009
Publisher: CSIR
Abstract: Sodium borohydride (SBH) reduction of isocoumarins has been effected in presence of methanol to their respective diols. Diols have been isolated, purified and characterized by GCMS, proton, carbon and two-dimensional NMR spectroscopy analysis. Complete NMR assignments of diols are made using H–H COSY, as well as HSQC, HMQC and HMBC heteronuclear correlation techniques.
Description: 825-832
URI: http://hdl.handle.net/123456789/4547
ISSN: 0376-4699
Appears in Collections:IJC-B Vol.48B(06) [June 2009]

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