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Title: Synthesis and characterization of dibutylgermanium(IV) dialkylthiophosphates
Authors: Garje, Shivram S
Mokal, Vijaya B
Jain, VimaI K
Issue Date: Oct-1995
Publisher: NISCAIR-CSIR, India
Abstract: The reaction of dibutylgermanium dichloride with two molar equivalents of ammonium dialkylthiophosphates in benzene. yields dibutylgermanium bis(dialkylthiophosphates), [Bu”2Ge{(OSP(OR)2}2] (R=Et, Pr", Pr', Bu").The latter complexes have been characterized by phosphorus analysis, IR and NMR (1H, 13C and 31P) data. The spectroscopic data suggest that these complexes contain four-coordinate germanium with monodentate dialkylthiophosphate ligand.
Page(s): 809-810
ISSN: 0975-0975(Online); 0376-4710(Print)
Appears in Collections:IJC-A Vol.34A(10) [October 1995]

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