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Title: A facile and efficient microwave-mediated <i>S</i>-alkylation of thiophosphates
Authors: Pandey, Lokesh Kumar
Mazumder, Avik
Pathak, Uma
Keywords: Microwave
<i style="">S</i>-alkylated thiophosphate
alkyl halides
<i style="">O, O’</i>-dialkyl thiophosphates
Issue Date: Apr-2009
Publisher: CSIR
Abstract: A convenient, highly efficient, safe microwave-mediated <i>S</i>-alkylation of <i style="">O,O’-</i>dialkyl thiophosphate has been reported. Clean and rapid <i>S</i>-alkylation of thiophosphates can be achieved by irradiating a mixture of dialkylthiophosphate salt and alkyl halide under microwave for a brief period. Alkylation occurs exclusively at sulfur to provide <i style="">S</i>-alkylated products. Through a simple workup, pure compounds have been obtained easily in good yields.<i style=""></i>
Description: 602-605
ISSN: 0376-4699
Appears in Collections:IJC-B Vol.48B(04) [April 2009]

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