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|Title:||A facile and efficient microwave-mediated S-alkylation of thiophosphates|
|Authors:||Pandey, Lokesh Kumar|
|Keywords:||Microwave;S-alkylated thiophosphate;alkyl halides;O, O’-dialkyl thiophosphates|
|Abstract:||A convenient, highly efficient, safe microwave-mediated S-alkylation of O,O’-dialkyl thiophosphate has been reported. Clean and rapid S-alkylation of thiophosphates can be achieved by irradiating a mixture of dialkylthiophosphate salt and alkyl halide under microwave for a brief period. Alkylation occurs exclusively at sulfur to provide S-alkylated products. Through a simple workup, pure compounds have been obtained easily in good yields.|
|Appears in Collections:||IJC-B Vol.48B(04) [April 2009]|
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