NISCAIR Online Periodicals Repository

Research Journals >
Indian Journal of Chemistry -Section A (IJC-A) >
IJC-A Vol.46A [2007] >
IJC-A Vol.46A(10) [October 2007] >

Title: Spectrophotometric determination of nickel(II) with 2-hydroxy-3-methoxy-benzaldehyde thiosemicarbazone
Authors: Kumar, A Praveen
Reddy, P Raveendra
Reddy, V Krishna
Issue Date: Oct-2007
Publisher: CSIR
IPC CodeInt. Cl. ⁸ G01N21/25
Abstract: 2-Hydroxy-3-methoxy benzaldehyde thiosemicarbazone has been synthesized, characterized and its analytical application investigated. It reacts with nickel(II) in aqueous solution at pH 4.0-8.0 and at room temperature to form a yellow coloured ML (1:1) complex with absorption maximum at 410 nm and molar absorptivity 2.0510⁴ l mol⁻¹ cm⁻¹. Beer’s law is obeyed in the range of 0.058-2.347 μg ml⁻¹ of Ni(II). A method for the determination of nickel(II) by second order derivative spectrophotometry has also been proposed. Interference of various diverse ions has been studied. The proposed methods have been successfully applied to determination of nickel in aluminium-based steels, drinking water, plant samples and in vegetable oil.
Page(s): 1625-1629
ISSN: 0376-4710
Source:IJC-A Vol.46A(10) [October 2007]

Files in This Item:

File Description SizeFormat
IJCA 46A(10) 1625-1629.pdf123.3 kBAdobe PDFView/Open
 Current Page Visits: 1228 
Recommend this item


Online Submission of Articles |  NISCAIR Website |  National Knowledge Resources Consortium |  Contact us |  Feedback

Disclaimer: NISCAIR assumes no responsibility for the statements and opinions advanced by contributors. The editorial staff in its work of examining papers received for publication is helped, in an honorary capacity, by many distinguished engineers and scientists.

CC License Except where otherwise noted, the Articles on this site are licensed under Creative Commons License: CC Attribution-Noncommercial-No Derivative Works 2.5 India

Copyright © 2015 The Council of Scientific and Industrial Research, New Delhi. All rights reserved.

Powered by DSpace Copyright © 2002-2007 MIT and Hewlett-Packard | Compliant to OAI-PMH V 2.0

Home Page Total Visits: 162379 since 01-Sep-2015  Last updated on 21-Jun-2016Webmaster: