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Title: Preparation, crystal structure and thermal decomposition of phenylenediammonium dichloride salts
Authors: Kapoor, Inder Pal Singh
Srivastava, Pratibha
Singh, Gurdip
Issue Date: Aug-2007
Publisher: CSIR
Abstract: Phenylene-1,2-diammonium dichloride (P-1,2-DADCl), phe¬nylene-1,3-diammonium dichloride (P-1,3-DADCl), phenylene-1,4-diammonium dichloride (P-1,4-DADCl) and 5-carboxyl-phe¬nylene-1,3-diammonium dichloride (5-carboxyl-P-1,3-DADCl) salts have been prepared and characterized by elemental, spectral, gravimetric and X-ray crystallography. Thermal decomposition of these salts has been studied by TG and DSC and shows involvement of proton transfer as a primary step. Kinetic analysis of TG data has been evaluated by model fitting method and model free isoconversional methods.
Page(s): 1277-1282
ISSN: 0376-4710
Appears in Collections:IJC-A Vol.46A(08) [August 2007]

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