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Title: Ultrasound promoted synthesis of (±)-8-hydroxy-5-isopropyl-8-methyl-6(E)nonen- 2-one ((±)-solanone hydrate) and 3,7-dimethyl -2(E),7-octadienylpropionate
Authors: Singh, Vasundhara
Chaudhary, Sangeeta
Sapehiyia, Varinder
Kaur, Irvinder
Kad, Goverdhan Lal
Singh, Jasvinder
Issue Date: Sep-2004
Publisher: NISCAIR-CSIR, India
IPC Code: Int.Cl.7 C 07 C
Abstract: A facile synthesis of the title compounds has been accomplished using Zn-Cu couple catalyzed conjugate addition of allylic halides to α, β-unsaturated ketones initiated by ultrasonic waves under aqueous conditions and Horner-Wittig reaction using ethyl α-dimethylphosphonoacetate and NaH as base in dry THF as the key steps in overall good yields.
Page(s): 1950-1953
ISSN: 0975-0983(Online); 0376-4699(Print)
Appears in Collections:IJC-B Vol.43B(09) [September 2004]

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