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Title: Thenoyltrifluoroacetone as a spectrophotometric reagent for determination of ascorbic acid
Authors: Arya, Satya Prakash
Jain, Preeti
Issue Date: Oct-2003
Publisher: NISCAIR-CSIR, India
Abstract: An extractive spectrophotometric method for the determination of microamounts of ascorbic acid is described.1-[Thenoyl- (2')-3,3,3-trifluoro-acetone] (HTTA) is found to react with iron (III) in strongly acidic medium giving a red coloured complex. The method is based on the proportionate decrease in the colour intensity of Fe(III)-HTTA complex with the addition of ascorbic acid at 405 nm. Linear calibration curve is observed in the range 1.0-5.0 μg/mL of ascorbic acid. The molar absorptivity and Sandell's sensitivity are 5.3×104 L/mol/cm and 0.003μg/cm2, respectively. The interference of sugars, vitamins, amino acids, mineral salts, sweetening agents etc. has been studied. The method is success fully used in the determination of ascorbic acid in pure vitamin C tablets, drops and multivitamin products.
Page(s): 2541-2544
ISSN: 0975-0975(Online); 0376-4710(Print)
Appears in Collections:IJC-A Vol.42A(10) [October 2003]

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