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Title: Solvent free diacetylation of aldehydes using a solid acid under microwave irradiation and a simple route to their regeneration
Authors: Barua, Akashi
Das, Pranab J
Keywords: Protection;Deprotection;Aldehydes;1,1-diacetates;Solid state reaction;Surfactant
Issue Date: Jun-2008
Publisher: CSIR
Abstract: A simple solvent-free microwave mediated procedure for the selective protection of aldehydes by conversion to their 1,1-diacetates is reported. The resultant diacetates were deprotected to generate the aldehyde using aqueous formic acid in the presence of a surfactant in high yield.
Page(s): 938-941
ISSN: 0376-4699
Appears in Collections:IJC-B Vol.47B(06) [June 2008]

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