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|Title:||Solvent free diacetylation of aldehydes using a solid acid under microwave irradiation and a simple route to their regeneration|
Das, Pranab J
|Keywords:||Protection;Deprotection;Aldehydes;1,1-diacetates;Solid state reaction;Surfactant|
|Abstract:||A simple solvent-free microwave mediated procedure for the selective protection of aldehydes by conversion to their 1,1-diacetates is reported. The resultant diacetates were deprotected to generate the aldehyde using aqueous formic acid in the presence of a surfactant in high yield.|
|Appears in Collections:||IJC-B Vol.47B(06) [June 2008]|
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