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Indian Journal of Chemistry -Section B (IJC-B) >
IJC-B Vol.51B [2012] >
IJC-B Vol.51B(02) [February 2012] >
| Title: | Synthesis of 6-aryl-9-(4-hydroxy-3-ethoxyphenyl)-1,2,4-triazolo [4,3-a][1,8]naphthyridines under microwave irradiation |
| Authors: | Mogilaiah, K Jagadeeshwar, K Rao, A Nageswara |
| Keywords: | 1,8-Naphthyridine 1,2,4-Triazole Silicagel Supported Ferric Chloride (SiO2-FeCl3) Solvent-Free Conditions Microwave Irradiation |
| Issue Date: | Feb-2012 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | A simple and
efficient method for the synthesis of 6-aryl-9-(4-hydroxy-3-ethoxyphenyl)-1,2,4-triazolo[4,3-a][1,8]
naphthyridÂines 4 by the
oxidation of the corresponding ethylvanillin
3-aryl-1,8-naphthyridin-2-ylhydrazones 3 using silicagel supported ferric chloride (SiO2-FeCl3) in solvent-free conditions under microwave
irradiation has been described. The products are obtained in good yields and in
a state of high purity. The structural assignment of compounds 3 and
4 were based on their elemental analyses and spectral data. |
| Page(s): | 398-401 |
| CC License: | CC Attribution-Noncommercial-No Derivative Works 2.5 India |
| Source: | IJC-B Vol.51B(02) [February 2012]
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