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NPARR Vol.2 [2011] >
NPARR Vol.2(2) [April 2011] >
| Title: | Analytical Methods |
| Issue Date: | Apr-2011 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | High-performance liquid chromatographic method with diode-array detection (HPLC–DAD) was optimised and validated for determination of tetracyclines (TCs) residue in chicken meat and liver through evaluating each step of various methods. The principle steps involved ultrasonic-assisted extractionof TCs from chicken samples by 2 ml of 20% trichloroacetic acid and citrate buffer (pH 4) which gave a clearer supernatant and high recovery, followed by centrifugation and purification on SPE (Strata C18-E cartridge) using 10 ml of 0.01 M methanolic oxalic acid for TCs elution. |
| Page(s): | 118-119 |
| CC License: |  CC Attribution-Noncommercial-No Derivative Works 2.5 India |
| Source: | NPARR Vol.2(2) [April 2011]
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